Thiophenes

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Room-Temperature Direct β-Arylation of Thiophenes and Benzo[b]thiophenes and Kinetic Evidence for a Heck-type Pathway

The first example of a regioselective β-arylation of benzo[b]thiophenes and thiophenes at room temperature with aryl iodides as coupling partners is reported. This methodology stands out for its operational simplicity: no prefunctionalization of either starting material is required, the reaction is insensitive to air and moisture, and it proceeds at room temperature. The mild conditions afford ...

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Thiophenes of Tagetes Flowers and Partial Purification of Xanthophyll Esters

Lutein is a health promoting xanthophyll that may be extracted from marigold flowers. But the plant is known also for biosynthesis of phototoxic polythiophenes. Extracts of flowers of some Tagetes species grown in Belgorod (RF) T. erecta L. (cv. Gavaii) , T. patula L. (cv. Petit orange), T. tenuifolia Cav. (unknown cv.), and T. lucida Cav. were investigated by thin layer chromatography (TLC) an...

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Activation of Thiophenes by Superacids: Protonation and Polymerization

Two aspects of thiophene chemistry are of current interest in materials chemistry. Polythiophenes are under intense study for possible applications in electronics and photonics,1 and metal-thiophene interactions are relevant to the catalytic hydrodesulfurization (HDS) process.2,3 This communication presents studies at the interface of these otherwise distinct topics, resulting from an examinati...

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Facilitated transport of thiophenes through Ag2O-filled PDMS membranes

Facilitated transport membranes of polydimethylsiloxane (PDMS) with silver oxide (Ag2O) as the carrier were prepared and used for the separation of thiophenes/n-octane mixtures. The effect of the degree of Ag2O loading, feed temperature on the pervaporation properties of Ag2O-filled membranes was investigated experimentally. Ag2O-filling leads to an increase in selectivity to thiophenes but a d...

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Palladium-catalysed direct arylation of thiophenes tolerant to silyl groups.

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ژورنال

عنوان ژورنال: Synthesis

سال: 2006

ISSN: 0039-7881,1437-210X

DOI: 10.1055/s-2006-958168